QuantaSmart™ - 国立大学法人...

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QuantaSmart™ Tri-Carb® ᾮయࢩࢳࢩࢼࢨ ᾮయࢩࢳࢩࢼࢨ ᾮయࢩࢳࢩࢼࢨ ᾮయࢩࢳࢩࢼࢨ Model 2810TR, 2910TR, 3110TR, 3180TR/SL

Transcript of QuantaSmart™ - 国立大学法人...

  • QuantaSmart™

    Tri-Carb®

    Model 2810TR, 2910TR, 3110TR, 3180TR/SL

  • 1

    1

    1

    Online Help 1

    5

    5

    6

    Library 12

    2

    15

    15

    16

    17

    17

    18

    18

    Getting Started 19

    3

    IPA 21

    21

    21

    IPA 21

    21

    IPA 23

    IPA 29

  • 4

    CPM 33

    CPM 33

    CPM 34

    Assay Definition 35

    Assay Parameters 36

    Count Conditions 38

    Count Corrections 41

    Report Definition 43

    Report Output 46

    Special Files 47

    Worklist 49

    5

    50

    50

    51

    52

    52

    52

    Output 53

    6

    54

    54

    54

    55

    56

    Assay Definition 57

    Assay Parameters 58

    Count Conditions 60

    Count Corrections 63

    Report Definition 65

    Report Output 68

    Special Files 69

    Worklist 71

  • 7

    DPM 73

    DPM 73

    DPM 74

    Assay Definition 75

    Assay Parameters 76

    Count Conditions 78

    Count Corrections 83

    Report Definition 85

    Report Output 88

    Special Files 89

    Worklist 91

  • QuantaSmart

    Operation manual 1

    1

    QuantaSmart Tri-Carb

    Windows Xp

    Output Report Spectra View

    Replay

    Nuclide Library

    QuantaSmart

    Online Help

    QuantaSmart

    QuantaSmart Help

    Contents, Index, search help text link

    QuantaSmart Help

  • QuantaSmart

    Operation manual 2

    Contents

    Contents

    Figure 1-1. Contents

  • QuantaSmart

    Operation manual 3

    Index

    Index

    Figure 1-2. Index

  • QuantaSmart

    Operation manual 4

    Find “Word” “Words”

    “Word” Word

    Note “Word” “Phrase” “Help”

    Find

    Figure 1-3. Find

  • QuantaSmart

    Operation manual 5

    Assay

    QuantaSmart

    Assay Definition

    Protocol

    QuantaSmart 60

    60

  • QuantaSmart

    Operation manual 6

    QuantaSmart

    File Run View Libraries Tools IPA Diagnostics

    Help

    Figure 1-4.

  • QuantaSmart

    Operation manual 7

    Alt

    File

    File

    Run

    Run

    View

    View

    “Replay” View

    Libraries

    Libraries “Sample Nuclides” “Quench Standards Libraries”

    “Alpha Beta”

    “Alpha Beta” “Alpha Beta Standard”

    Tool

    Tool “Radio nuclide Decay Calculator”

    IPA

    IPA (Instrument Performance Assessment )

    Diagnostics

    Diagnostics

  • QuantaSmart

    Operation manual 8

    Window

    “Spectra View”

    Help

    Help QuantaSmart

    Instrument Status Bar

    Status Bar

    Protocol Tree

    Protocol Tree

    Flags

    “Priostat ”

  • QuantaSmart

    Operation manual 9

    Report Symbol

    Prohibitory Symbols

    “Nuclide

    Library”

    The Replay Tree

    “Replay” “Replay Tree”

  • QuantaSmart

    Operation manual 10

    SpectraView

    1.

    2.

    3.

    4.

    Figure 1-5. SpectraView .

  • QuantaSmart

    Operation manual 11

    Sample Number

    Count time

    Pre-count Delay

    Note

    Acquisition Time

    Apply AEC

    tSIE AEC

    AEC Automatic Efficiency Correction

    AEC

    KeV Full Scale

    “Auto”

    Count Full Scale

    Y

    “Auto”

    Y

    Log keV Scale

    Log keV

  • QuantaSmart

    Operation manual 12

    Linear keV Scale

    keV

    Region

    RegionA,B,C

    CPM

    CPM

    CPM

    2%S

    95% Confidence limits

    Assay Definition

    Report Definition

    Library

    “Nuclide Library” “Nuclide Library”

    “Alpha Beta”

    “Alpha Beta” “Alpha Beta Nuclide

    Library”

    “Quench Standard Library”

    “DPM Assay” DPM Disintegration Per Minute

  • QuantaSmart

    Operation manual 13

    “Sample Nuclide Library”

    “Alpha Beta Standard” “Alpha Beta Nuclide Library” “Quench Standard”

    “Sample Nuclides Library”

    “Alpha Beta Assay”

    “Library” “Library ”

  • QuantaSmart

    Operation manual 14

    - Note -

  • QuantaSmart

    Operation manual 15

    2

    β

    CPM Count Per Minute

    DPM Disintegration Per Minute

    DPM

  • QuantaSmart

    Operation manual 16

    Figure 2-1.

    4ml

    12 15 20ml 18

    6 7ml

    ID ID

    PID Positive Sample Identification

    Toward

  • QuantaSmart

    Operation manual 17

    DPM

    Run

    Pause Stop

    Start Resume

    Next Protocol

    End Protocol

    Forward

    Reverse

  • QuantaSmart

    Operation manual 18

    QuantaSmart “Assay Definition”

    “Reports”

    Protocol

    Protocol

    Output

    File Print

    Assay Select Assay

    OK

  • QuantaSmart

    Operation manual 19

    Getting Started

    Alpha Beta, Alpha Beta Standards, CPM Assay, DPM

    Single, DPM Dual, DPM Triple, FS DPM, Direct DPM, Quench Standards,

    Single Photo Counting

    Direct DPM DPM

    3 7

  • QuantaSmart

    Operation manual 20

    - Note -

  • QuantaSmart

    Operation manual 21

    IPA

    (IPA)

    PMT

    14

    C

    β

    14C QIP Quench Indicating

    Parameter SIE transformed Spectral Index of the External Standard

    1000 tSIE

    1000

    IPA

    IPA Instrument Performance Assessment3H

    14C

    Figure of Merit2

    Chi-Square

    IPA

    SNC Self-Normalization & Calibration IPA

    SNC 23

  • QuantaSmart

    Operation manual 22

    Note BGO

    IPA 23 SNC

    23

    SNC IPA

    23 SNC IPA

    IPA 23

    IPA

    23

  • QuantaSmart

    Operation manual 23

    IPA

    IPA

    IPA IPA Definition

    IPA Definition

    Figure 3-1. IPA Definition

    3H Standard DPM

    3H DPM

    ( ) DPM

  • QuantaSmart

    Operation manual 24

    3H Reference Date

    3H

    14C -14 Standard DPM

    14C DPM

    DPM

    14C

    Background Count Time

    14C

    3H

    60

    3H E

    2B Figure of Merit Threshold

    E2

    B E2

    B

    IPA

    14C -14 E

    2B Figure of Merit Threshold

    14C E

    2B E

    2

    IPA

    Do Chi Square Test for 3H

    20

  • QuantaSmart

    Operation manual 25

    Do Chi Square Test for 14C -14

    -14

    14C 20

    RS 232 Transmit IPA Data

    IPA RS 232

    of Datapoints to Establish Baseline

    14C IPA

    99

    3H Background Mean and Limit

    IPA

    4SE

    14C -14 Background Mean and Limit

    IPA14

    C

    4SE

    3H Efficiency Mean and Limit

    IPA

    3%

    14C -14 Efficiency Mean and Limit

    IPA -14

    3%

  • QuantaSmart

    Operation manual 26

    Reset Baselines

    IPA

    Establish Baseline 99

    Super Low Level SNC

    IPA

    SNC

    Note SNC

    Figure 3-2. Super Low Level Tri-Carb SNC

    -14

    High Sensitivity Low Level super Low Level

  • QuantaSmart

    Operation manual 27

    “IDLE”

    SNC

    IPA

    “ ”

    Super Low Level BGO SNC

    IPA

    SNC

    Note SNC

  • QuantaSmart

    Operation manual 28

    Figure 3-3. Super Low Level Tri-Carb SNC

    2. 14

    C

    3.

    4. 3H

    5.

    6. IDLE

    SNC

    IPA

    “ ”

    Note BGO

    IPA 23 SNC

  • QuantaSmart

    Operation manual 29

    IPA

    IPA IPA IPA

    IPA

    IPA

    IPA

    IPA

    IPA

    14C -14 Background

    -14 IPA

    SD

    SD IPA

    14C -14 Background Baseline

    -14

    “IPA Definition”

    14C -14 Chi-Square

    -14 IPA

    30 20

    7.63 36.19

    SD IPA

    14C -14 Efficiency

    -14

    SD IPA

  • QuantaSmart

    Operation manual 30

    14C -14 Efficiency Baseline

    IPA Definition

    14C -14 Figure of Merit

    FOM Figure of Merit

    14 SD

    IPA

    3H Background

    IPA

    SD Standard Deviation

    SD IPA

    3H Background Baseline

    IPA Deviation

    SD Standard Deviation

    3H Chi Square

    IPA

    30 20

    7.63 36.19

    SD IPA

    3H Efficiency

    SD IPA

  • QuantaSmart

    Operation manual 31

    3H Efficiency Baseline

    IPA Definition

    3H Figure of Merit

    FOM Figure of Merit

    SD

    IPA

    IPA

    IPA

    IPA

    Figure 3-4. IPA Charts & Tables Window

  • QuantaSmart

    Operation manual 32

    - Note -

  • QuantaSmart

    Operation manual 33

    CPM

    CPM

    QuantaSmart

    CPM

    CPM

    1 2 3

    CPM Count Per

    Minute

    CPM

    3

  • QuantaSmart

    Operation manual 34

    CPM

    CPM File New Assay

    Select Assay Type (Figure 4-1)

    Figure 4-1. Select Assay Type

    Select Assay Type CPM OK Assay

    Definition (Figure 4-2)

    Note: QuantaSmart

  • QuantaSmart

    Operation manual 35

    Assay Definition

    Assay Definition Assay Parameters, Count Conditions, Count

    Corrections, Report Definition, Report Output, Special Files, Worklist

    Assay Definition

    CPM

    ■

    ■ Sample Nuclides library

    ■

    ■

    ■

    ■ Worklist

  • QuantaSmart

    Operation manual 36

    Assay Parameters

    Assay Parameters

    Figure 4-2. Assay Parameters Tab

    Password

    Lock Assay

    Note

    Lock Assay

    Password

  • QuantaSmart

    Operation manual 37

    Author

    Assay Description

    Note: ”Assay Parameters”

  • QuantaSmart

    Operation manual 38

    Count Conditions

    Count Conditions

    Figure 4-3. Count Conditions Tab

    Name

    Sample Nuclide Library

    (Figure 4-4)

  • QuantaSmart

    Operation manual 39

    Figure 4-4. Sample Nuclides Library

    Note:

    Sample Nuclide Library

    Sample Nuclide Library

    DPM

    OK

    Assay Count Cycles

    Count Time

    2 Sigma% Low Count Reject (LCR)

  • QuantaSmart

    Operation manual 40

    Background Subtract

    CPM

    st

    10 CPM

    IPA IPA

    IPA

    CPM

    Note: Count Conditions ”Count

    Conditions”

  • QuantaSmart

    Operation manual 41

    Count Corrections

    Count Corrections

    Figure 4-5. Count Corrections Tab

    Static Controller

    -

    ■ 40%

    ■ (PPN 7000901)

    ■

    Pre-Count delay

  • QuantaSmart

    Operation manual 42

    Luminescence Correction

    Apply Half-life Correction

    Sample Nuclide Library

    Reference Date Time Reference Date Time

    Note: Count Correction ”Count Correction”

  • QuantaSmart

    Operation manual 43

    Report Definition

    Report Definition

    Figure 4-6. Report Definition Tab

    Report Name

    Report Name

    Note: /,@,

  • QuantaSmart

    Operation manual 44

    Report Fields

    Report Fields

    Report Fields

    Report Fields Block

    Data

    Add

    Report Fields custom

    Delete

    Note: (Custom) Custom

    Format

    Equation…

    custum

    Note Delete Note

  • QuantaSmart

    Operation manual 45

    Figure 4-7. Equation

  • QuantaSmart

    Operation manual 46

    Report Output

    Report Output

    Figure 4-8. Report Output

    Report Output

    RS-232

    Note: QuantaSmart

    Delimited Text ASCII Excel Lotus 1-2-3

  • QuantaSmart

    Operation manual 47

    Special Files

    Special Files

    Figure 4-9. Special Files

    ■ Spectra File (composite) 1

    ■ Spectrum File (Individual) 1

    ■ IPA Data File

    ■ Prot.dat file

    ■ 2000ca.dat file

    Data Output Path

  • QuantaSmart

    Operation manual 48

    Assay Parameter Assay Definition OK

    5

  • QuantaSmart

    Operation manual 49

    Worklist :

    Assay Definition Worklist ( 4-10) Positive Identification (PID#)

    Sample List Library

    Note Worklist

    Note Worklist 2810TR, 2910TR 3110TR, 3180TR

    Figure 4-10. Worklist Tab.

  • QuantaSmart

    Operation manual 50

    1. 3

    2. Assay Definition 5

    4,6,7

    3.

    QuantaSmart

    Associate

    Assay… File Associate Assay

    Figure 5-1.

  • QuantaSmart

    Operation manual 51

    Associate Assay

    Data Paths User ID Additional Header

    OK Protocol

    Figure 5-2.

    forward

  • QuantaSmart

    Operation manual 52

    QuantaSmart Figure

    5-1

    Output Figure 5-3

    Print

  • QuantaSmart

    Operation manual 53

    Output

    Output Figure 5-3

    Assay Definition 5

    Assay Definition Output

    Figure 5-3. Output

  • QuantaSmart

    Operation manual 54

    QuantaSmart

    2

    (QIP) SIS, tSIE

    %Efficiency vs QIP DPM

    (Disintegration Per Minute) DPM CPM Efficiency

  • QuantaSmart

    Operation manual 55

    1

    DPM

    DPM=CPM/Efficiency

    3 ”Calibration”

  • QuantaSmart

    Operation manual 56

    File New Assay

    Assay

    Type

    Figure 6-1. Select Assay Type

    Assay Type Quench Standards OK Assay

    Definition

    Note: QuantaSmart

  • QuantaSmart

    Operation manual 57

    Assay Definition

    Assay Definition Assay Parameters, Count Conditions, Count

    Corrections, Report Definition, Report Output, Special Files Worklist

    Assay Definition

    CPM

    ■

    ■ Sample Nuclides Library

    ■

    ■

    ■

    ■ Worklist

  • QuantaSmart

    Operation manual 58

    Assay Parameters

    Assay Parameters

    Figure 6-2. Assay Parameters Tab

    Password

    Lock Assay

    Lock Assay

    Password

    Author

  • QuantaSmart

    Operation manual 59

    Assay Description

    Note: ”Assay Parameters”

  • QuantaSmart

    Operation manual 60

    Count Conditions

    Count Conditions

    Figure 6-3. Count Conditions Tab

    Name

    Quench Standard Library

    (Figure 6-4)

  • QuantaSmart

    Operation manual 61

    Figure 6-4. Quench Standards Library

    Quench Standard Quench Standard Library

    Quench Standard Library

    DPM DPM

    DPM DPM

    ( )

    DPM Reference Date

    QuantSmart DPM

    OK

    Note:

    Quench Standard Library Quench Curve

    ”Quench Curve”

  • QuantaSmart

    Operation manual 62

    Count Time

    2 Sigma% Low Count Reject (LCR)

    Background Subtract

    CPM

    st

    10 CPM

    IPA IPA

    IPA

    CPM

    Note: Count Conditions ”Count

    Conditions”

  • QuantaSmart

    Operation manual 63

    Count Corrections

    Count Corrections

    Figure 6-5. Count Corrections Tab

    Static Controller

    -

    ■ 40%

    ■ (PPN 7000901)

    ■

    Pre-Count delay

  • QuantaSmart

    Operation manual 64

    Apply Half-life Correction

    Quench Standard Library

    Reference Date Time Reference Date

    Time

    DPM

    DPM

    Note: Count Correction ”Count Correction”

  • QuantaSmart

    Operation manual 65

    Report Definition

    Report Definition

    Figure 6-6. Reports Tab

    Report Name

    Report Name

    Note: /,@,

  • QuantaSmart

    Operation manual 66

    Report Fields

    Report Fields

    Report Fields

    Report Fields Block

    Data

    Add

    Report Fields custom

    Delete

    Note: (Custom) Custom

    Format

    Equation…

    custum

    Note Delete Note

  • QuantaSmart

    Operation manual 67

    Figure 6-7. Equation

  • QuantaSmart

    Operation manual 68

    Report Output

    Report Output

    Figure 6-8. Report Output

    Report Output

    RS-232

  • QuantaSmart

    Operation manual 69

    Special Files

    Special Files

    Figure 6-9. Special Files

    ■ Spectra File (composite) 1

    ■ Spectrum File (Individual) 1

    ■ IPA Data file

    ■ Prot.dat file

    ■ 2000ca.dat file

    Data Output Path

  • QuantaSmart

    Operation manual 70

    Quench Standard

    Library DPM

    Assay Parameter Assay Definition OK

    5

  • QuantaSmart

    Operation manual 71

    Worklist :

    Assay Definition Worklist ( 6-10) Positive Identification (PID#)

    Sample List Library

    Note Worklist

    Note Worklist 2810TR, 2910TR 3110TR, 3180TR

    Figure 6-10. Worklist Tab.

  • QuantaSmart

    Operation manual 72

    - Note -

  • QuantaSmart

    Operation manual 73

    DPM

    DPM

    2 DPM

    DPM

    DPM

    DPM DPM

    DPM

    DPM

    ■ CPM

    ■ (QIP)

    ■ (%Efficiency vs. QIP)

    ■ DPM CPM Efficiency DPM

    DPM

    1. 2

    ”Calibration”

    2. DPM

    6 ”Quench

    Standard Assay”

  • QuantaSmart

    Operation manual 74

    DPM

    DPM File New Assay

    Select Assay Type (Figure 7-1)

    Figure 7-1. Select Assay Type

    Select Assay Type DPM(Single) OK

    Assay Definition

    Note: QuantSmart

  • QuantaSmart

    Operation manual 75

    Assay Definition

    Assay Definition Assay Parameters, Count Conditions, Count

    Corrections, Report Definition, Report Output, Special Files Worklist

    Assay Definition

    CPM

    ■

    ■ Sample Nuclides library

    ■

    ■

    ■

    ■ Worklist

  • QuantaSmart

    Operation manual 76

    Assay Parameters

    Assay Parameters

    Figure 7-2. Assay Parameters Tab

    Password

    Lock Assay

    Lock Assay

    Password

    Author

  • QuantaSmart

    Operation manual 77

    Assay Description

    Note: ”Assay Parameters”

  • QuantaSmart

    Operation manual 78

    Count Conditions

    Count Conditions

    Figure 7-3. Count Conditions Tab

    Name

    Sample Nuclide Library

    (Figure 7-4)

  • QuantaSmart

    Operation manual 79

    Figure 7-4. Sample Nuclides Library

    Note:

    Sample Nuclide Library

    Sample Nuclide Library

    Quench Set

    Quench Set 1 1

    Low Quench 2

    2 Medium Set 3

    3 High Set Quench Standard

    (Figure 7-5)

  • QuantaSmart

    Operation manual 80

    Figure 7-5. Quench Standards Library

    DPM OK

    Sample Nuclide Library Quench Set

    Assay Definition Count Conditions Quench Set

    (Figure 7-3)

    Sample Nuclide Library OK

  • QuantaSmart

    Operation manual 81

    Quench Indicator

    Quench Indicator Parameter 3

    tSIE(transformed Spectral Index of External standards)

    Barium-133

    tSIE tSIE

    1000 tSIE

    10 DPM

    160,000 0.5% 2Sigma tSIE

    tSIE/AEC AEC

    SIS SIS

    SIS CPM

    Assay Count Cycles

    Count Time

    2 Sigma% Low Count Reject (LCR)

  • QuantaSmart

    Operation manual 82

    Background Subtract

    CPM

    st

    10 CPM

    IPA IPA

    IPA

    CPM

    Note: Count Conditions ”Count

    Conditions”

  • QuantaSmart

    Operation manual 83

    Count Corrections

    Count Corrections

    Figure 7-6. Count Corrections Tab

    Static Controller

    -

    ■ 40%

    ■ (PPN 7000901)

    ■

    Pre-Count delay

  • QuantaSmart

    Operation manual 84

    Luminescence Correction

    Apply Half-life Correction

    Sample Nuclide Library

    Reference Date Time Reference Date

    Time

    Note: Count Correction ”Count Correction”

  • QuantaSmart

    Operation manual 85

    Report Definition

    Report Definition

    Figure 7-7. Reports Tab

    Report Name

    Report Name

    Note: /,@,

  • QuantaSmart

    Operation manual 86

    Report Fields

    Report Fields

    Report Fields

    Report Fields Block

    Data

    Add

    Report Fields custom

    Delete

    Note: (Custom) Custom

    Format

    Equation…

    custum

    Note Delete Note

  • QuantaSmart

    Operation manual 87

    Figure 7-8. Equation

    Note:

  • QuantaSmart

    Operation manual 88

    Report Output

    Report Output

    Figure 7-9. Report Output

    Report Output

    RS-232

  • QuantaSmart

    Operation manual 89

    Special Files

    Special Files

    Figure 7-10. Special Files

    ■ Spectra File (Composite) 1

    ■ Spectrum File (Individual) 1

    ■ IPA Data file

    ■ Prot.dat file

    ■ 2000ca.dat file

  • QuantaSmart

    Operation manual 90

    Assay Parameter Assay Definition OK

    5

  • QuantaSmart

    Operation manual 91

    Worklist :

    Assay Definition Worklist ( 7-11) Positive Identification (PID#)

    Sample List Library

    Note Worklist

    Note Worklist 2810TR, 2910TR 3110TR, 3180TR

    Figure 7-11. Worklist Tab.

  • QuantaSmart

    Operation manual 92

    ― Note

    QuantaSmart表紙QuantaSmart目次QuantaSmartマニュアル


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ККАК РЕАЛИЗОВАТЬ АК РЕАЛИЗОВАТЬ …...1 CPM — Corporate Performance Management. синонимы CPM — Enterprise Performance Management (EPM), Strategic

ККАК РЕАЛИЗОВАТЬ АК РЕАЛИЗОВАТЬ …...1 CPM — Corporate Performance Management. синонимы CPM — Enterprise Performance Management (EPM), Strategic

Cahier des modules spécialité CPM

Cahier des modules spécialité CPM

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F: ulletinactivite ul199908A99 · 2019. 5. 20. · P 86/99 µ µ ( , 3 µ 1999) µ µ µ RCD (Rassemblement Congolais pour ... 01.09.99 C4-0717/98 ROCARD ( ) 01.09.99 C4-0219/99 BLOKLAND

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La newsletter des utilisateurs - Apicrypt€¦ · }À} µ µv }oo u ] µ ]8 ]o u v u` ] o Uu] o[W/ Dv À}µoµ v v o i µ ]vPr }vP }uuµv] µ µ ]( }o u] µ X Assistance technique

La newsletter des utilisateurs - Apicrypt€¦ · }À} µ µv }oo u ] µ ]8 ]o u v u` ] o Uu] o[W/ Dv À}µoµ v v o i µ ]vPr }vP }uuµv] µ µ ]( }o u] µ X Assistance technique

Paques 2017-FINAL Enregistré automatiquement...h h v } ] À ] À v P À } µ i W > W/d d/KE Z µ v v v } µ À } µ } o o ] ] } v } µ o ] ] } v µ ] v } µ o o À ( } v v o [ v

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Isabelle.Bloch@enst.fr bloch · XestA et Y estB µ A∧B(x,y) = t[µ A(x),µ B(y)] • Disjonction XestA ou Y estB µ A∨B(x,y) = T[µ A(x),µ B(y)] • Négation µ¬A(x) = c[µ

[email protected] bloch · XestA et Y estB µ A∧B(x,y) = t[µ A(x),µ B(y)] • Disjonction XestA ou Y estB µ A∨B(x,y) = T[µ A(x),µ B(y)] • Négation µ¬A(x) = c[µ

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Pert cpm techniques

Pert cpm techniques